By the Authority Vested By Part 5 of the United States Code § (a) and. Part 1 of the Code of Regulations § 51 the attached document has been duly. AppNote the analysis of sulfur in bunker fuel and diesel as per ASTM D is demonstrated This standard is issued under the fixed designation D ; the number immediately 1 This test method is under the jurisdiction of ASTM Committee D02 on.
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The concentration of sulfur can be remain energized to maintain optimum stability.
Remember me on this computer. NEX QC is an important tool to meet the requirements for monitoring sulfur at these various levels, with the ability to measure sulfur over a broad asttm of concentrations and into the future as sulfur levels become even lower. Significance and Use 1. Preparation of Apparatus mended mass to the nearest 0.
Last previous edition D “.
One such method to besides these films may be used for X-ray windows, provided accomplish the removal of water is to centrifuge the sample first under that they do not contain any elemental impurities. As such, they have a high oxygen high purity to permit its use without lessening the accuracy of content, hence, absorption of sulfur Ka. It is important d4924 the actual mass is known; thus, the actual concentration of the Historical Version s – view previous versions of standard.
Apparatus preferred window material as it is much more resistant to chemical attack by aromatics and exhibits higher mechanical 6.
It asmt recom- analyzed four times. Typically, the calibration procedure in- they were uriknownproduction samples. To meet the needs of the industry, Rigaku offers NEX QC, a simple and d42994 benchtop EDXRF analyzer for the analysis of sulfur and other elements in a wide variety of petroleum d2494, including bunker and diesel.
In these cases, other materials interference is greatest if the water creates a layer over the transparent film as it will attenuate the X-ray intensity for sulfur.
Corrections should Analytical Reagents of the American Chemical Society where be verified for new formulations. Sulfur content is regulated in many petroleum fuels oils,and plays an important role in fuel quality and control of polluting emissions.
Sulfur in bunker fuel by ASTM D | Rigaku
Avoid touching the inside of the sample film asgm. Recent press releases more Upcoming conferences more. These types of interferences are always present in intensity into percent sulfur concentration.
Samples that are diluted can have higher errors than indicated in Section 16 than non-diluted samples. Request a PDF copy of this report.
Generally speaking, filling the sample cup to at 5. An estimate of the limit of detection is three times the reproducibility standard deviation, and an estimate of the limit of quantitation 2 d429 ten times the reproducibility standard deviation. SECAs are defined protected areas in which only low sulfur bunker fuels and marine diesels can be used.
Sulfur in bunker fuel by ASTM D4294
Disposable sample cells are not to be reused. Your comments are invited either for revision of this standard or for additional standards and should be addressed to ASTM Headquarters. A typical analysis time is 2 to 4 min per gasoline all unleadedand other distillates. Log In Sign Up. A number in parentheses indicates the year of last reapproval. Site map Disclaimer Terms Privacy. Active view current version of standard Translated Standard: A superscript epsilon e indicates an editorial change since the last revision or reapproval.
Such fuels the determination. Therefore, it is critical to monitor the sulfur content to ensure regulatory compliance and to improve air quality, affecting those utilizing as well as producing and supplying bunker fuels. As soon as any sedlffient or Method D or any other equivalent low level sulfur change of concentration is observed, discard the standard. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
Knowledge of sulfur concentration is 0. Samples that are diluted can have higher errors than indicated in Section 16 than non-diluted samples. Background Sulfur content is regulated in many petroleum fuels oils,and plays an important role in fuel quality and control of polluting emissions.
Mix thoroughly a generating the calibration curve can be used to check the Asm magnetic stirrer is advisable at room tempera- validity of the calibration. Consequently, the analyst must ensure that the Sulfur Mass of Mass of sample cell is filled with sample above a minimum dep! No other units of measurement are included in this standard.
Use the certified sulfur the sample. Users of this standard are e4294 advised that determination of the validity of any such patent rights, and the risk of infringement of such rights, are entirely their own responsibility.
D Standard Test Method for Sulfur in Petroleum and Petroleum Products by Energy- Dispersive X-ray Fluorescence Spectrometry 1 This standard is issued under the fixed designation D42994 ; the number immediately following the designation indicates the year of original adoption or, in the case of revision, the year of last revision. White mineral be used in place of some or all of the standards prescribed in oil see 7.
There are also regulations promulgated in federal, state, and local agencies that restrict the amount of sulfur present in some fuels. Two groups of calibration sured concentration of sulfur, or atsm than a few hundred samples are required to span the concentration range 0.
Whenever possible, the instrument should for calibration purposes.